HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → 1-(Naphthalen-2-yl)ethan-1-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | N-[1-(2-Naphthalenyl)ethyl]formamide | HCID 18543124 | — |
| Solvent | Water | HCID 962 | — |
| Product | 1-(Naphthalen-2-yl)ethan-1-amine | HCID 3857145 | 98.7% |
Reaction Steps
A mixture of N-(1-naphthalen-2-yl-ethyl)-formamide (1.12 g), ethanol (10 mL) and 5 N sodium hydroxide (10 mL) is heated at reflux for 1 hour. The solution is cooled, poured into water and extracted with ether. The ether solution is dried with anhydrous potassium carbonate, filtered and concentrated to give the product (0.95 g) as a pale yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06255349B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-f1e56aec2feb456cbbc092edb8234aea |
| Source note | uspto-grants-2001_07 |