HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Trifluoroacetylphenol → [2-[2-(N-Dodecyl-N-methylamino)ethoxy]phenyl]-2,2,2-trifluoroethanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Trifluoroacetylphenol | HCID 2761164 | — |
| Reactant | Dodecyl(2-hydroxyethyl)methylamine | HCID 10657884 | — |
| Product | [2-[2-(N-Dodecyl-N-methylamino)ethoxy]phenyl]-2,2,2-trifluoroethanone | HCID 18319145 | 61.2% |
Reaction Steps
2-Trifluoroacetylphenol (Matsumoto, S.; Kobayashi, H. and Ueno, K. Bull. Chem. Soc. Jpn. 1969, 42, 960) (490 mg, 2.57 mmol) and 2-[N-dodecyl-N-methylamino] ethanol (627 mg, 2.58 mmol) were reacted by the general procedure as described in example 1 and afforded the title compound (654 mg, 61%) as a pale yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06255496B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-e01239760fc14bd2aada696da08cc869 |
| Source note | uspto-grants-2001_07 |