HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Ethyl-1-butanol → 2-Fluoro-4-acetoxy-1-(2-ethylbutyloxy)carbonylbenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Ethyl-1-butanol | HCID 7358 | — |
| Reactant | 4-Acetoxy-2-fluorobenzoic acid | HCID 22721416 | — |
| Reactant | CID 57465351 | HCID 57465351 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | 2-Fluoro-4-acetoxy-1-(2-ethylbutyloxy)carbonylbenzene | HCID 21185477 | — |
Reaction Steps
Thionyl chlorine in an amount of 60 ml (milliliter) was added to 11.9 g (0.06 mol) of 2-fluoro-4-acetoxybenzoic acid, and the mixture was allowed to react under reflux for 7 hours. Then, excess thionyl chloride was distilled off, and then 10 ml of pyridine and 3.7 g (0.0402 mol) of 2-ethyl-1-butanol were dropwise added.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06258296B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-77dd2ee3a0bc4451bae19c9baf507115 |
| Source note | uspto-grants-2001_07 |