Benzaldehyde, 2-ethoxy- → HCID 85049630, compound

HRID 1384382Notes

Reaction equation

HRID 1384382 reaction equation
[CH2:1]([O:3][C:4]1[CH:11]=[CH:10][CH:9]=[CH:8][C:5]=1[CH:6]=O)[CH3:2].[CH:12]1([NH:17][OH:18])[CH2:16][CH2:15][CH2:14][CH2:13]1>>[CH2:1]([O:3][C:4]1[CH:11]=[CH:10][CH:9]=[CH:8][C:5]=1[CH:6]=[N+:17]([CH:12]1[CH2:16][CH2:15][CH2:14][CH2:13]1)[O-:18])[CH3:2]

Participants

3

Reactant 2

HCID 11950Benzaldehyde, 2-ethoxy-HCID 10219393N-cyclopentylhydroxylamine

Product 1

HCID 85049630HCID 85049630, compoundYield 72.6%

Procedure

Using 2-ethoxybenzaldehyde and N-cyclopentylhydroxylamine and following the procedures described herein, the title compound was obtained in 72.6% yield as white crystals, m.p. 87.3° C. (Rf=0.43 on a silica gel plate using hexanes:EtOAc, 2: 1, v:v, as an eluant).

Sources & evidence

ORD record
ord-fd2ce99b0e1641d699f5188b3bd4d8f1
Source dataset
uspto-grants-2001_07
Patent number
US06258852B1

Reaction notes

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