Gamma-undecalactone → Sodium 4-hydroxyundecanoate

Participants

Reaction Steps

To a solution of 43.6 g of sodium hydroxide in 150 ml of methanol heated to reflux, 200 g of gamma-undecalactone was dropped in. After stirring for 2 hours at reflux, the mixture was cooled to room temperature and evaporated to dryness. The resulting crystals were washed with hexane to yield 240 g of colorless crystals.

Provenance & Evidence