HuagongsheHuagongshe Chemistry Print Report · For research reference only
Fumaronitrile → 2-(2,6-Dichloro-4-trifluoromethylphenylhydrazino)succinonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Fumaronitrile | HCID 637930 | — |
| Reactant | [2,6-Dichloro-4-(trifluoromethyl)phenyl]hydrazine | HCID 688223 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Solvent | Water | HCID 962 | — |
| Product | 2-(2,6-Dichloro-4-trifluoromethylphenylhydrazino)succinonitrile | HCID 53933941 | — |
Reaction Conditions
| Temperature | 100 °C |
|---|
Reaction Steps
A mixture of 2,6-dichloro-4-trifluoromethylphenylhydrazine (1.0 g) and fumaronitrile (1.0 g) in dimethylsulfoxide (10 ml) was heated at 100° C. for 7 hours. The cooled mixture was diluted with water and extracted (ether) to give, after evaporation and crystallization from dichloromethane/hexane, the title compound (0.828 g, 63%), m.p. 101-102° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06258973B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-354d5861b8424fd79a9ed8aba10df099 |
| Source note | uspto-grants-2001_07 |