HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → HCID 12298995, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | Ethyl 5-methyl-1,2,3-thiadiazole-4-carboxylate | HCID 351614 | — |
| Product | HCID 12298995 | HCID 12298995 | — |
Reaction Steps
Hydrolysis of ethyl 5-methyl-1,2,3-thiadiazole-4-carboxylate (D. L. Pain and R. Sleck, J. Chem. Soc., 5166 (1965)) and subsequent treatment of the acid with oxalyl chloride according to the method of Example 3 provides 5-methyl-1,2,3-thiadiazole-4-carbonyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06262059B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-220589a7cd3c4be7999151e430ef2863 |
| Source note | uspto-grants-2001_07 |