Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | 3-Aminobenzoic Acid | HCID 7419 | — |
| Reactant | Acrylonitrile | HCID 7855 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 18403024 | HCID 18403024 | — |
Reaction Steps
200.0 g of 3-aminobenzoic acid in 2 l of water were admixed with 53.2 g of sodium hydroxide. At 30° C., 126.6 g of acrylonitrile were added dropwise, and the mixture was then heated under reflux for 22 hours. The mixture was then cooled to 5° C. and acetic acid was added (pH=5) and the precipitate which had formed was filtered off with suction and washed with water.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06262074B1 |
|---|
| Source dataset | uspto-grants-2001_07 |
|---|
| ORD ID | ord-c5a379447d674622ae901a99621e4d19 |
|---|
| Source note | uspto-grants-2001_07 |
|---|
