HCID 18545957, compound → HCID 18545876, compound

HRID 1385084Notes

Reaction equation

HRID 1385084 reaction equation
[Cl:1][C:2]1[CH:10]=[C:9]2[C:5]([C:6]([C:11]3[CH2:12][CH2:13][N:14]([CH2:17][CH2:18][C:19]([N:21]4[C:29]5[C:24](=[CH:25][CH:26]=[CH:27][CH:28]=5)[CH2:23][CH2:22]4)=O)[CH2:15][CH:16]=3)=[CH:7][NH:8]2)=[CH:4][CH:3]=1.[H-].[H-].[H-].[H-].[Li+].[Al+3]>>[Cl:1][C:2]1[CH:10]=[C:9]2[C:5]([C:6]([C:11]3[CH2:12][CH2:13][N:14]([CH2:17][CH2:18][CH2:19][N:21]4[C:29]5[C:24](=[CH:25][CH:26]=[CH:27][CH:28]=5)[CH2:23][CH2:22]4)[CH2:15][CH:16]=3)=[CH:7][NH:8]2)=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 18545957HCID 18545957, compoundHCID 21226445Aluminium lithium hydride

Product 1

HCID 18545876HCID 18545876, compound

Procedure

The compound was prepared from 41a as described in Example 11 but by the use of alane instead of LiAlH4 for the reduction.

Sources & evidence

ORD record
ord-71b7570fa90040fe85c94261e4bdad59
Source dataset
uspto-grants-2001_07
Patent number
US06262087B1

Reaction notes

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