HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 21183709, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 54059647 | HCID 54059647 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 21183709 | HCID 21183709 | — |
Reaction Steps
This compound was prepared according to the method of Example 1.D, starting with 3.28 g (13.4 mmol) 2-cyclopentyl-2H-indazole-6-carboxylic acid methyl ester, 100 mL CH3OH and 40 mL 1N NaOH, to give 2.71 g (88%) of light yellow powder: mp 190-193° C.; Anal. calcd for C13H14N2O2: C, 67.79; H, 6.13; N, 12.16. Found: C, 67.40; H, 6.04; N, 12.38.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06262040B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-131477ce954f4cdf99540baa6bd8a7ac |
| Source note | uspto-grants-2001_07 |