HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Aminoquinoline → 1-Cyclopentyl-3-ethyl-N-5-quinolinyl-1H-indazole-6-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Aminoquinoline | HCID 11911 | — |
| Reactant | HCID 15545850 | HCID 15545850 | — |
| Product | 1-Cyclopentyl-3-ethyl-N-5-quinolinyl-1H-indazole-6-carboxamide | HCID 15547424 | 30% |
Reaction Steps
This compound was prepared according to the method of Example 15, using 91 mg (0.329 mmol, 1.0 equiv) 1-cyclopentyl-3-ethyl-1H-indazole-6-carbonyl chloride and 52 mg (0.362 mmol, 1.1 equiv) 5-amino-quinoline as starting materials, to give 38 mg (30%) of pale yellow powder: mp 176-178° C.; Anal. calcd for C24H24N4O: C, 74.96; H, 6.29; N, 14.57. Found: C, 74.33; H, 6.53; N, 14.31.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06262040B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-78eb3db099554a57aa520e94a84cfec0 |
| Source note | uspto-grants-2001_07 |