HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyloxyamine hydrochloride → HCID 53875714, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyloxyamine hydrochloride | HCID 102312 | — |
| Reactant | HCID 21183687 | HCID 21183687 | — |
| Product | HCID 53875714 | HCID 53875714 | 72% |
Reaction Steps
This compound was prepared according to the method of Example 37, using 250 mg (0.759 mmol, 1.0 equiv) 3-[(1-cyclopentyl-3-ethyl-1H-indazole-6-carbonyl)-amino]-propionic acid and 121 mg (0.759 mmol, 1.0 equiv) O-benzylhydroxylamine hydrochloride as starting materials, to give 237 mg (72%) of a white solid: mp 134-136° C.; Anal. calcd for C25H30N4O3: C, 69.10; H, 6.96; N, 12.89. Found: C, 69.36; H, 6.75; N, 12.85.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06262040B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-6c673c4fd184413db29d4fb3c5e8d4ae |
| Source note | uspto-grants-2001_07 |