HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylboronic Acid → HCID 21183701, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylboronic Acid | HCID 66827 | — |
| Reactant | HCID 22733808 | HCID 22733808 | — |
| Product | HCID 21183701 | HCID 21183701 | 77.2% |
Reaction Steps
This compound was prepared according to the method of Example 55, using 128 mg (0.437 mmol, 1.0 equiv) 6-bromo-1-cyclopentyl-3-ethyl-1H-indazole and 75 mg (0.612 mmol, 1.4 equiv) phenyl boronic acid as starting materials, to give 98 mg (77%) of white crystals: mp 72-74° C.; Anal. calcd for C20H22N2: C, 82.77; H, 7.64; N, 9.65. Found: C, 81.95; H, 7.82; N, 9.75.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06262040B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-63975a9f926146478db1f5d3c769fbbf |
| Source note | uspto-grants-2001_07 |