HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methoxyphenyl isocyanate → N-(2-Hydroxy-4-nitrophenyl)-N'-(3-methoxyphenyl)urea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methoxyphenyl isocyanate | HCID 87843 | — |
| Reactant | 2-Amino-5-Nitrophenol | HCID 4984721 | — |
| Product | N-(2-Hydroxy-4-nitrophenyl)-N'-(3-methoxyphenyl)urea | HCID 21184674 | 46.2% |
Reaction Steps
N-(2-Hydroxy-4-nitrophenyl)-N′-(3-methoxyphenyl)urea was prepared from 2-hydroxy 4-nitro aniline (154 mg, 1.0 mmol) and 3-methoxy phenyl isocyanate (1.0 mmol) according to the procedure in General Method B. The product was purified by dilution with methylene chloride and precipitation with hexanes. Filtering afforded the title compound (140 mg, 46%). EI-MS m/z 302 (M−H)−
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06262113B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-e64663e71b0c4d20bfd4b941fff362be |
| Source note | uspto-grants-2001_07 |