HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromophenyl isocyanate → HCID 22011327, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromophenyl isocyanate | HCID 137097 | — |
| Reactant | HCID 54436784 | HCID 54436784 | — |
| Product | HCID 22011327 | HCID 22011327 | 24% |
Reaction Steps
The urea was synthesized from 2-[(4-acetamidophenyl)sulfonylamino]phenyl aniline (1 mmol) and 2-bromo phenyl isocyanate (1 mmol) by general Method B. It was purified by dilution with methylene chloride and precipitation with hexane. Filtering afforded the desired compound (0.12 g, 24%). EI-MS m/z 501 (M−H)−
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06262113B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-1771b4864f7d484e81fad46a68485bb9 |
| Source note | uspto-grants-2001_07 |