反应详情

A mixture of 3.7 g of 16, 5.6 g (0.026 mole) of pyridinium chlorochromate, 2 g of Celite and 30 mL of methylene chloride was stirred for 18 h and filtered through a bed of silica gel. The silica gel was eluted with methylene chloride. The combined methylene chloride eluant was purified by HPLC (20% ETOAc-hexane) to give 2.4 g (66%) of an oil.

1. filtrationfiltered through a bed of silica gel
2. washThe silica gel was eluted with methylene chloride
3. customThe combined methylene chloride eluant was purified by HPLC (20% ETOAc-hexane)