HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 2,6-Difluorobenzene-1-carbothioamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 2,6-Difluorobenzonitrile | HCID 74695 | — |
| Reactant | Sodium sulfide monohydrate | HCID 19906495 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | 2,6-Difluorobenzene-1-carbothioamide | HCID 12683212 | — |
Reaction Steps
As illustrated in step a of Scheme III, 2,6-difluorobenzonitrile is reacted with triethylamine, sodium sulfide hydrate, and hydrochloric acid in pyridine at room temperature to give 2,6-difluorobenzenethioamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06262305B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-bd532648f6604cc29797a4e79623f9b3 |
| Source note | uspto-grants-2001_07 |