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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1386000Generated: November 2, 2026

1,1-Dimethoxyethyl(dimethyl)amine → HCID 18176643, compound

https://huagongshe.com/reaction/1386000

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1,1-Dimethoxyethyl(dimethyl)amineHCID 87835—
Reactant6-[[4-[3-(Trifluoromethyl)-phenoxy]butyl]thio]-3-pyridazinecarbothioamideHCID 18176642—
SolventTolueneHCID 1140—
ProductHCID 18176643HCID 18176643100%

Reaction Steps

A mixture of intermediate 12 (0.009 mol) and N,N-dimethylacetamide dimethyl acetal (0.015 mol) in toluene (100 ml) was stirred and refluxed for 3 hours. The solvent was evaporated, yielding 4.1 g (100%) of N-[1-(dimethylamino)ethylidene]-6-[[4-[3-(trifluoromethyl)phenoxy]butyl]thio]-3-pyridazinecarbothioamide (intermediate 13).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06265407B1
Source datasetuspto-grants-2001_07
ORD IDord-685f9b4a43ea40499ced41524933298a
Source noteuspto-grants-2001_07