1-Naphthalenesulfonyl chloride → HCID 21717142, compound

HRID 1386023Notes

Reaction equation

HRID 1386023 reaction equation
[Cl:1][CH2:2][CH2:3][CH:4]1[CH2:9]C[CH2:7][CH2:6][N:5]1[S:10]([C:13]1[C:22]2[C:17](=[CH:18][CH:19]=[CH:20][CH:21]=2)[CH:16]=[CH:15][CH:14]=1)(=[O:12])=[O:11].OCCC1C[S:30]CCN1.C1(S(Cl)(=O)=O)C2C(=CC=CC=2)C=CC=1>>[Cl:1][CH2:2][CH2:3][CH:4]1[CH2:9][S:30][CH2:7][CH2:6][N:5]1[S:10]([C:13]1[C:22]2[C:17](=[CH:18][CH:19]=[CH:20][CH:21]=2)[CH:16]=[CH:15][CH:14]=1)(=[O:12])=[O:11]

Participants

4

Reactant 3

HCID 665601-Naphthalenesulfonyl chlorideHCID 21717133HCID 21717133, compoundHCID 21717136HCID 21717136, compound

Product 1

HCID 21717142HCID 21717142, compoundYield 70%

Procedure

The title compound (300 mg, 70%) was prepared according to the procedure outlined in D1 using 3-(2-hydroxyethyl)thiomorpholine and 1-naphthalenesulfonyl chloride.

Sources & evidence

ORD record
ord-aafa7fafd51d45269836ee738a16a9ec
Source dataset
uspto-grants-2001_07
Patent number
US06265408B1

Reaction notes

Loading…