HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methylimidazole → 6-[2-(2-Methyl-imidazole-1-yl)-ethoxy]-3,4-dihydro-2H-naphthalen-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methylimidazole | HCID 12749 | — |
| Reactant | 6-(beta-Chloroethoxy)-1-tetralone | HCID 12042982 | — |
| Product | 6-[2-(2-Methyl-imidazole-1-yl)-ethoxy]-3,4-dihydro-2H-naphthalen-1-one | HCID 18626528 | 66% |
Reaction Steps
According to the method of Example 1, Step 2, 6-(β-chloroethoxy)-1-tetralone (0.208 g, 0.93 mmol) and 2-methylimidazole (0.137 g, 1.67 mmol) were reacted to provide the title compound (0.166 g, 66%) as a cream colored solid: CI-MS m/e 270 (M+), 271 (M++1);
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06265422B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-fa6d28a9d8a44685ac973dd2e1d9f16e |
| Source note | uspto-grants-2001_07 |