HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 178472654, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 178472655 | HCID 178472655 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 178472654 | HCID 178472654 | — |
Reaction Steps
In 50 ml of methylene chloride was dissolved 2.73 g (8.40 mmol) of ethyl 5-t-butoxycarbonyl-3-hydroxy-4,5,6,7-tetrahydropyrazolo[4,3-c]pyridin-2-acetate, and under ice-cooling, 10 ml of CF3CO2H was added to the solution and the mixture was stirred at room temperature for 2 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06265418B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-e48a1f0b50b04b59ab00dbbdd74e1685 |
| Source note | uspto-grants-2001_07 |