HCID 9883327, compound → HCID 21182010, compound

HRID 1386472Notes

Reaction equation

HRID 1386472 reaction equation
[CH3:1][C:2]1[CH:23]=[CH:22][CH:21]=[CH:20][C:3]=1[O:4][CH2:5][CH2:6][N:7]([CH2:9][CH2:10][C:11]1[CH:16]=[CH:15][C:14]([N+:17]([O-])=O)=[CH:13][CH:12]=1)[CH3:8]>C(OCC)(=O)C.CO>[CH3:8][N:7]([CH2:9][CH2:10][C:11]1[CH:12]=[CH:13][C:14]([NH2:17])=[CH:15][CH:16]=1)[CH2:6][CH2:5][O:4][C:3]1[CH:20]=[CH:21][CH:22]=[CH:23][C:2]=1[CH3:1]

Participants

3

Reactant 1

HCID 9883327HCID 9883327, compound

Product 1

HCID 21182010HCID 21182010, compound

Reagents, catalysts & solvents 1

HCID 21584119Ethylacetate methanolSolvent

Procedure

The title compound is prepared as described in Example 7, except that N-[2-(2-methylphenoxy)ethyl]-N-methyl-2-(4-nitrophenyl)ethylamine (Example 3) is used as starting material to obtain a yield of 82% of the base (oil), Rf=0.35 (ethyl acetate/methanol=9:1).

Sources & evidence

ORD record
ord-dc8f71e7df024fb48c5d4d5ab0f9114c
Source dataset
uspto-grants-2001_07
Patent number
US06265445B1

Reaction notes

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