HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl cyanoacetate → HCID 273843, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl cyanoacetate | HCID 7764 | — |
| Reactant | Cyclopropyl methyl ketone | HCID 13004 | — |
| Product | HCID 273843 | HCID 273843 | 29% |
Reaction Steps
A solution of 118 g (1.4 mol) of cyclopropyl methyl ketone and 113 g (1 mol) of ethyl cyanoacetate was reacted by a method similar to Example 3a) to give 50 g (yield 29%) of ethyl 2-cyano-3-cyclopropylbut-2-enoate (b.p. 105° C./6 mbar).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06265447B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-90a03576a02e431b9fd024f3eca9a3df |
| Source note | uspto-grants-2001_07 |