HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21182397, compound → HCID 21182438, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21182397 | HCID 21182397 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Platinum oxide (PtO) | HCID 82844 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 21182438 | HCID 21182438 | 96.2% |
Reaction Steps
A mixture of Methyl 6-(1-heptynyl)naphthalene-2-carboxylate (4.51 g) and platinum oxide (0.4 g) in tetrahydrofuran was stirred under 3.5 atm pressure of hydrogen for 5 hours. The catalyst was filtered off and the filtlate was evaporated to give Methyl 6-heptylnaphthalene-2-carboxylate (4.40 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06265536B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-0e44f53fcc014024a695e8ad5caa9aa5 |
| Source note | uspto-grants-2001_07 |