HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → (3-Carboxypropyl)(triphenyl)phosphanium chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | 3-Chloropropionic acid | HCID 7899 | — |
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Product | (3-Carboxypropyl)(triphenyl)phosphanium chloride | HCID 21180642 | 95% |
Reaction Steps
A solution of 1 g (9.2 mmol) of 3-chloropropanoic acid and 2.4 g (9.2 mmol) of triphenylphosphine was refluxed in 10 mL of toluene overnight. After cooling, the mixture was concentrated to give 3.25 g (95%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06265434B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-004f87a1d66044389876ac9e54b3777d |
| Source note | uspto-grants-2001_07 |