HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 53804942, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1,3-Diiodopropane | HCID 12314 | — |
| Reactant | N-(4-Hydroxyphenyl)-5-methyl-1,2-oxazole-4-carboxamide | HCID 19439747 | — |
| Product | HCID 53804942 | HCID 53804942 | — |
Reaction Steps
6.5 g (0.03 mol) of 5-methylisoxazole-4-carboxylic acid (4-hydroxyphenyl)amide are dissolved in 57 ml (0.5 mol) of 1,3-diiodopropane and 26.2 g (0.19 mol) of finely ground potassium carbonate are added with intensive stirring. The reaction is complete after approximately 4 h. Working up is carried out by means of filtration, concentration and chromatography on silica gel by means of ethyl acetate/petroleum ether 1:1 with addition of 1% glacial acetic acid. The yield of the process was 6.7 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06265588B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-5e2b4484594241b88abc525754992300 |
| Source note | uspto-grants-2001_07 |