p-Anisoyl chloride → HCID 10667130, compound

HRID 1386969Notes

Reaction equation

HRID 1386969 reaction equation
[C:1](Cl)(=[O:10])[C:2]1[CH:7]=[CH:6][C:5]([O:8][CH3:9])=[CH:4][CH:3]=1.[CH3:12][O:13][C:14]1[CH:19]=[CH:18][C:17]([C:20]2[S:24][C:23]3[CH:25]=[CH:26][CH:27]=[CH:28][C:22]=3[CH:21]=2)=[CH:16][CH:15]=1>>[CH3:9][O:8][C:5]1[CH:6]=[CH:7][C:2]([C:1]([C:21]2[C:22]3[CH:28]=[CH:27][CH:26]=[CH:25][C:23]=3[S:24][C:20]=2[C:17]2[CH:16]=[CH:15][C:14]([O:13][CH3:12])=[CH:19][CH:18]=2)=[O:10])=[CH:3][CH:4]=1

Participants

3

Reactant 2

HCID 7477p-Anisoyl chlorideHCID 41373912-(4-Methoxyphenyl)benzothiophene

Product 1

HCID 10667130HCID 10667130, compoundYield 90%

Procedure

The title compound was prepared from 4-anisoyl chloride and 2-(4-methoxyphenyl)benzo[b]thiophene (Part A) as a tan solid in 90% yield following recrystallization from THF-hexanes.

Workup

  1. customrecrystallization from THF-hexanes

Sources & evidence

ORD record
ord-724ba795ed384801ab0547141bc1f0ef
Source dataset
uspto-grants-2001_07
Patent number
US06265575B1

Reaction notes

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