HuagongsheHuagongshe Chemistry Print Report · For research reference only
(4-Methoxyphenyl)boronic acid → 2-(4-Methoxyphenyl)-3-(4-methoxyphenoxy)benzo[b]thiophene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (4-Methoxyphenyl)boronic acid | HCID 201262 | — |
| Reactant | 2-Iodo-3-(4-methoxyphenoxy)benzo[b]thiophene | HCID 10691279 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 2-(4-Methoxyphenyl)-3-(4-methoxyphenoxy)benzo[b]thiophene | HCID 11793004 | 70% |
Reaction Steps
By essentially following the procedure detailed in Example 1, Part B, the title compound was prepared from 2-iodo-3-(4-methoxyphenoxy)benzo[b]thiophene (Part B) and (4-methoxyphenyl)boronic acid (Part C) in 70% yield following chromatography (SiO2; 5% EtOAc in hexanes).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06265575B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-c0ce58324bd54ddb9494a30ba4e3b937 |
| Source note | uspto-grants-2001_07 |