HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalic Acid → HCID 86757212, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalic Acid | HCID 971 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | HCID 11801169 | HCID 11801169 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 86757212 | HCID 86757212 | 99% |
Reaction Steps
3-[[4-[2-(1-Piperidinyl)ethoxy]phenyl]methyl]-2-[4-[2-(1-pyrrolidinyl)ethoxy]phenyl]benzo[b]thiophene-6-methanamine (Part C) was dissolved in 50 mL of ethyl acetate and added to a solution of 100 mg of oxalic acid in 30 mL of ethyl acetate. After adding 10 mL of ether to the solution, the precipitate was filtered to give 1.05 g (99%) of a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06265575B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-27613f84c52043ff950f7e550676553d |
| Source note | uspto-grants-2001_07 |