HuagongsheHuagongshe Chemistry Print Report · For research reference only
rac-(1R,2R)-2-(dimethylamino)cyclohexan-1-ol → HCID 18397527, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | rac-(1R,2R)-2-(dimethylamino)cyclohexan-1-ol | HCID 15560793 | — |
| Reactant | HCID 21182699 | HCID 21182699 | — |
| Product | HCID 18397527 | HCID 18397527 | 77% |
Reaction Steps
The title compound was prepared in 77% yield by essentially following the procedures outlined in Example 72, Part E, from 4-fluorophenyl 6-methoxy-2-[4-[2-(1-pyrrolidinyl)ethoxy]phenyl]benzo[b]thiophen-3-yl ketone (Example 59, Part A) and (±)-trans-2-(dimethylamino)cyclohexanol (Part A).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06265575B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-f6d180f4607546e986c0b60b6b39550f |
| Source note | uspto-grants-2001_07 |