HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 178527215, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-Chlorobenzene-1-carboperoxoic acid | HCID 12587398 | — |
| Reactant | 3-Phenylpropyl 3-(1H-imidazol-4-yl)propyl sulphide | HCID 178420274 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 178527215 | HCID 178527215 | — |
Reaction Steps
0.5 g of potassium carbonate in 40 ml of dichloromethane are added to 2 mmol of the compound obtained in Example 46 and the mixture is stirred for 30 min. 2.5 mmol of chloroperbenzoic acid in 20 ml of dichloromethane are slowly added to the suspension and the mixture is stirred for 2 h at room temperature. The suspension is filtered and purification is carried out by chromatography. The title compound is recrystallized in the hydrogenmaleate form from ethanol/diethyl ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | USRE037303E1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-4ace6c9ba7304e99b506723b7fc64d33 |
| Source note | uspto-grants-2001_07 |