HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → HCID 68819508, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | HCID 68828182 | HCID 68828182 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 68819508 | HCID 68819508 | — |
Reaction Steps
A solution of 6-1 (380 mg, 1.0 mmol), p-TSA (20 mg) and acetone (50 mL) was heated at reflux for 4 hr. The cooled reaction mixture was diluted with EtOAc and then washed with sat. NaHCO3 and brine, dried (MgSO4), and concentrated to afford 6-2 as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06268378B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-5627d714a4a04c1896b6e4a35bf99f67 |
| Source note | uspto-grants-2001_07 |