HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 70234942, compound → HCID 70234419, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 70234942 | HCID 70234942 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 70234419 | HCID 70234419 | — |
Reaction Steps
A mixture of 6-3 (380 mg, 0.8 mmol) and 10% Pd/carbon (200 mg) in EtOH (20 mL) was stirred under a balloon of hydrogen for 6 h. Following filtration and evaporative removal of the solvent, the residue was chromatographed (silica gel, 70:25:5 to 70:20:10 chloroform/ethyl acetate/MeOH) to give 6-4 as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06268378B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-45a98a605fba4fdeb2b6db14f1430cd9 |
| Source note | uspto-grants-2001_07 |