HCID 21927910, compound → HCID 21934585, compound

HRID 1387446Notes

Reaction equation

HRID 1387446 reaction equation
[N:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][N:9]=2)[CH:4]=[CH:3][C:2]=1[CH2:11][CH2:12][CH2:13][C:14]#[N:15].[H][H]>[Pd].C(O)C>[N:1]1[C:10]2[NH:9][CH2:8][CH2:7][CH2:6][C:5]=2[CH:4]=[CH:3][C:2]=1[CH2:11][CH2:12][CH2:13][C:14]#[N:15]

Participants

5

Reactant 2

HCID 21927910HCID 21927910, compoundHCID 178418361HCID 178418361, compound

Product 1

HCID 21934585HCID 21934585, compound

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 702EthanolSolvent

Procedure

A mixture of 8-2 (14 g, 71 mmol), 10% Pd/C (2 g) and ethanol (200 mL) was stirred under a balloon of hydrogen gas for 1 h. Filtration and evaporation produced 8-3 as a white solid.

Workup

  1. filtrationFiltration and evaporation

Sources & evidence

ORD record
ord-8bef0a32c0af4d9a8fa890520bdb9bed
Source dataset
uspto-grants-2001_07
Patent number
US06268378B1

Reaction notes

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