Methanol → HCID 17101926, compound

Participants

Reaction Steps

Prepared according to the procedure described for Example 10, Step A from 3,4-dichloro-N-3-nitro-4-fluorophenyl)-benzamide from Example 22, Step A (5.2 g, 20 mmol) and sodium (1.3 g, 57 mmol) using methanol in place of ethanol to afford the product (5.8 g). m.p. 215-218° C. after chromatography on silica gel in dichloromethane/methanol 99:1.

Provenance & Evidence