HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 18626090, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Veratraldehyde | HCID 8419 | — |
| Reactant | 3-Amino-4-methoxybenzanilide | HCID 8426 | — |
| Reactant | Sodium triacetoxyborohydride | HCID 5049666 | — |
| Product | HCID 18626090 | HCID 18626090 | 63.7% |
Reaction Steps
Prepared according to the procedure of Example 50 using 3,4-dimethoxybenzaldehyde (1.94 g, 11.6 mmol), 3-amino-4-methoxy-N-phenyl-benzamide (2.8 g, 11.6 mmol), acetic acid (0.69 g, 11.5 mmol), and sodium triacetoxyborohydride (2.6 g, 11.7 mmol) to afford the product (2.9 g); m.p. 187-188° C. after recrystallization from ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06268387B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-f6a06611f4094970a879a6ddb7ef325b |
| Source note | uspto-grants-2001_07 |