HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Aniline → 3-phenoxy-N-phenylbenzamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Aniline | HCID 6115 | — |
| Edukt | 3-Phenoxybenzoic acid | HCID 19539 | — |
| Edukt | Oxalyl chloride | HCID 65578 | — |
| Produkt | 3-phenoxy-N-phenylbenzamide | HCID 2465154 | 94,3% |
Reaktionsschritte
Prepared according to the procedure of Example 1 Step A using 3-phenoxybenzoic acid (1.2 g, 5.5 mmol), oxalyl chloride (0.55 mL, 6.3 mmol), and aniline (1.0 g, 10.7 mmol) to afford the product (1.5 g); m.p. 111-112° C. after recrystallization from ethanol.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06268387B1 |
| Quelldatensatz | uspto-grants-2001_07 |
| ORD ID | ord-dff6326775044e089bf1606e58dfa3b0 |
| Quellennotiz | uspto-grants-2001_07 |