3-Amino-4-methoxybenzanilide → HCID 54111046, compound

HRID 1387543Notes

Reaction equation

HRID 1387543 reaction equation
[NH2:1][C:2]1[CH:3]=[C:4]([CH:14]=[CH:15][C:16]=1[O:17][CH3:18])[C:5]([NH:7][C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1)=[O:6].[C:19]([C:22]1[CH:23]=[C:24]([N:28]=[C:29]=[S:30])[CH:25]=[CH:26][CH:27]=1)(=[O:21])[CH3:20]>>[C:19]([C:22]1[CH:23]=[C:24]([NH:28][C:29](=[S:30])[NH:1][C:2]2[CH:3]=[C:4]([CH:14]=[CH:15][C:16]=2[O:17][CH3:18])[C:5]([NH:7][C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)=[O:6])[CH:25]=[CH:26][CH:27]=1)(=[O:21])[CH3:20]

Participants

3

Reactant 2

HCID 84263-Amino-4-methoxybenzanilideHCID 5205153-Acetylphenylisothiocyanate

Product 1

HCID 54111046HCID 54111046, compoundYield 67.6%

Procedure

Prepared according to the procedure described for Example 60 using 3-amino-4-methoxy-N-phenyl-benzamide (0.971 g, 4.00 mmol) and 3-acetylphenyl isothiocyanate (0.709 g, 4.00 mmol) to afford the product (1.135 g); m.p. 176-177° C.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-b3acf5ef4b9a46758a53ae6c12f20a02
Source dataset
uspto-grants-2001_07
Patent number
US06268387B1

Reaction notes

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