HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Dichlorophenyl isothiocyanate → HCID 54090344, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Dichlorophenyl isothiocyanate | HCID 138776 | — |
| Reactant | HCID 18626050 | HCID 18626050 | — |
| Product | HCID 54090344 | HCID 54090344 | 74% |
Reaction Steps
Prepared according to the procedure described for Example 78 using 1-(4-methoxy-3-aminophenyl)-3-phenyl-urea from Example 24, Step C (0.390 g, 1.52 mmol) and 3,5-dichlorophenyl isothiocyanate (0.311 g, 1.52 mmol). Filtration without trituration afforded the product (0.5187 g); m.p. 218-219° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06268387B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-fa3aa9becdee414281b56fc44255c932 |
| Source note | uspto-grants-2001_07 |