HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Amino-4-methoxybenzanilide → 3-(Butane-1-sulfonylamino)-4-methoxy-N-phenyl-benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Amino-4-methoxybenzanilide | HCID 8426 | — |
| Reactant | 1-Butanesulfonyl chloride | HCID 75430 | — |
| Product | 3-(Butane-1-sulfonylamino)-4-methoxy-N-phenyl-benzamide | HCID 18626190 | 92% |
Reaction Steps
Prepared according to the procedure described for Example 128 using 1-butanesulfonyl chloride (0.47 g, 3.0 mmol) and 3-amino-4-methoxy-N-phenyl-benzamide (0.73 g, 3.0 mmol) to afford the product (1.0 g); m.p. 182-183° C. after recrystallization from ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06268387B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-dda7513d394a46579acf2a8215c7f513 |
| Source note | uspto-grants-2001_07 |