3-Amino-4-methoxybenzanilide → HCID 18626210, compound

HRID 1387579Notes

Reaction equation

HRID 1387579 reaction equation
[Cl:1][C:2]1[S:3][C:4]([Cl:11])=[CH:5][C:6]=1[S:7](Cl)(=[O:9])=[O:8].[NH2:12][C:13]1[CH:14]=[C:15]([CH:25]=[CH:26][C:27]=1[O:28][CH3:29])[C:16]([NH:18][C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1)=[O:17]>>[Cl:1][C:2]1[S:3][C:4]([Cl:11])=[CH:5][C:6]=1[S:7]([NH:12][C:13]1[CH:14]=[C:15]([CH:25]=[CH:26][C:27]=1[O:28][CH3:29])[C:16]([NH:18][C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1)=[O:17])(=[O:9])=[O:8]

Participants

3

Reactant 2

HCID 84263-Amino-4-methoxybenzanilideHCID 27360942,5-Dichlorothiophene-3-sulfonyl chloride

Product 1

HCID 18626210HCID 18626210, compoundYield 65.6%

Procedure

Prepared according to the procedure described for Example 127 using 2,5-dichlorothiophene-3-sulfonyl chloride (0.75 g, 3.0 mmol) and 3-amino-4-methoxy-N-phenyl-benzamide (0.73 g, 3.0 mmol) to afford the product (0.9 g); m.p. 189-190° C.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-c0369b85e4884026a0c9ba214ae2cc65
Source dataset
uspto-grants-2001_07
Patent number
US06268387B1

Reaction notes

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