HRID1387667

反应详情

EQUATION

反应方程式

HRID 1387667 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

CONDITIONS

反应条件

温度
20 °C

PROCEDURE

实验过程

To a solution of 2-Nitrophenyl isocyanate (3.34 g) in 100 mL of toluene was added aniline (2 g). The mixture was stirred at 20° C. for 30 min. Hexane (300 mL) was added and the resulting solid was filtered and dried to yield N-(2-Nitrophenyl)-N′-phenyl-urea as a light yellow solid.

WORKUP

后处理

  1. filtrationthe resulting solid was filtered
  2. customdried