HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18472611, compound → HCID 18472303, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18472611 | HCID 18472611 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 18472303 | HCID 18472303 | 99.6% |
Reaction Steps
A mixture of 4-nitrobenzyldiethylphosphine oxide (0.4 g) and 10% Pd—C (0.06 g) in ethanol (10 ml) was vigorously stirred under hydrogen atmosphere for 16 hours, and the Pd—C was filtered off. The filtrate was concentrated under reduced pressure to give 4-aminobenzyldiethylphosphine oxide (349 mg) as brown oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06268354B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-c8e6f05e15ac49c9aa6983f221ca2f4d |
| Source note | uspto-grants-2001_07 |