HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroquinone → HCID 53848281, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroquinone | HCID 785 | — |
| Reactant | Acrolein | HCID 7847 | — |
| Reactant | Hexadiene | HCID 11602 | — |
| Product | HCID 53848281 | HCID 53848281 | — |
Reaction Steps
A mixture of 1,3-hexadiene (cis/trans mixture, 20 g., 0.24 mole), acrolein (18 ml., 0.27 mole) and hydroquinone (50 mg.) was heated at 70°-75° C. for 22 hours. Distillation in vacuo gave purified title product (21.7 g.; b.p. 90° C./12-15 mm.; 78% cis, 22% trans by pnmr assay).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04430337 |
| Source dataset | uspto-grants-1984_02 |
| ORD ID | ord-99a88812ae7e41559aa0ac3930f9c531 |
| Source note | uspto-grants-1984_02 |