HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Chloroperbenzoic acid → HCID 53844734, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | HCID 53637641 | HCID 53637641 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 53844734 | HCID 53844734 | — |
Reaction Steps
2.4 g of the title compound, in the form of a colourless oil, which is purified by chromatography on silica gel (migrating agent: 90:10 petroleum ether/ethyl acetate), are obtained by the procedure described in Example 1a) from 4.9 g of 6-cyclohexyloxy-2-methylenehexanoic acid ethyl ester and 7 g of m-chloroperbenzoic acid in 50 ml of methylene chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04430339 |
| Source dataset | uspto-grants-1984_02 |
| ORD ID | ord-442207ff1c76409eaca72fd1c81a2f23 |
| Source note | uspto-grants-1984_02 |