HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Chloroperbenzoic acid → HCID 54054486, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | HCID 53918420 | HCID 53918420 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 54054486 | HCID 54054486 | — |
Reaction Steps
5.25 g of the title compound, in the form of a colourless oil, which is purified by chromatography on silica gel (migrating agent: 90:10 petroleum ether/ethyl acetate), are obtained by the procedure described in Example (1a) from 9.2 g of 9-cyclohexyl-2-methylenenonanoic acid ethyl ester and 11.3 g of m-chloroperbenzoic acid in 100 ml of methylene chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04430339 |
| Source dataset | uspto-grants-1984_02 |
| ORD ID | ord-795a31e4b271498aaba00eeb6cb0ed14 |
| Source note | uspto-grants-1984_02 |