HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Chloroperbenzoic acid → HCID 53852953, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | 8-Cyclopentyl-2-methyleneoctanoic acid ethyl ester | HCID 54242028 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 53852953 | HCID 53852953 | — |
Reaction Steps
5.33 g of the title compound, in the form of a nearly colourless oil, which is purified by chromatography on silica gel (migrating agent: 90:10 petroleum ether/ethyl acetate), are obtained by the procedure described in Example (1a) from 11.4 g of 8-cyclopentyl-2-methyleneoctanoic acid ethyl ester and 15.6 g of m-chloroperbenzoic acid in 120 ml of methylene chloride
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04430339 |
| Source dataset | uspto-grants-1984_02 |
| ORD ID | ord-3007463204824ed880a2c4b04cf44c45 |
| Source note | uspto-grants-1984_02 |