HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropanol → HCID 86739229, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropanol | HCID 3776 | — |
| Reactant | HCID 131713382 | HCID 131713382 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 86739229 | HCID 86739229 | — |
Reaction Steps
Using the procedure of Example 3, 6 g of (1R,cis) 2,2-dimethyl-3-[(E)-3-oxo-1-butenyl]-cyclopropane-1-carboxylic acid chloride and 2.7 ml of isopropanol were reacted to obtain 1.96 g of isopropyl (1R,cis) 2,2-dimethyl-3-[(E)-3-oxo-1-butenyl]-cyclopropane-1-carboxylate with a specific rotation of [α]D20 =-39°±5° (c=0.2% in benzene).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04431576 |
| Source dataset | uspto-grants-1984_02 |
| ORD ID | ord-0594edc5315b4d9ebb1d66e9a96b231e |
| Source note | uspto-grants-1984_02 |