HuagongsheHuagongshe Chemistry Print Report · For research reference only
O-Allylhydroxylamine hydrochloride → 2-Allyloxyimino-2-(3-chloro-4-hydroxyphenyl)acetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O-Allylhydroxylamine hydrochloride | HCID 3084724 | — |
| Reactant | 2-(3-Chloro-4-hydroxyphenyl)-2-oxoacetic acid | HCID 12961139 | — |
| Product | 2-Allyloxyimino-2-(3-chloro-4-hydroxyphenyl)acetic acid | HCID 136210784 | 98.1% |
Reaction Steps
2-(3-Chloro-4-hydroxyphenyl)glyoxylic acid (2 g.) and O-allylhydroxylamine hydrochloride (1.1 g.) were reacted according to a similar manner to that of Preparation 5-(2)(a) to give oil of 2-allyloxyimino-2-(3-chloro-4-hydroxyphenyl)acetic acid (syn isomer) (2.5 g.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04431643 |
| Source dataset | uspto-grants-1984_02 |
| ORD ID | ord-2c172b2820994a0a8b787c151a0046ef |
| Source note | uspto-grants-1984_02 |