HuagongsheHuagongshe Chemistry Print Report · For research reference only
Selenium Dioxide → Ethyl 2-(2-t-pentyloxycarbonylamino-1,3-thiazol-4-yl)glyoxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Selenium Dioxide | HCID 24007 | — |
| Reactant | Ethyl 2-(2-t-pentyloxycarbonylamino-1,3-thiazol-4-yl)acetate | HCID 19978738 | — |
| Product | Ethyl 2-(2-t-pentyloxycarbonylamino-1,3-thiazol-4-yl)glyoxylate | HCID 19978748 | 70.6% |
Reaction Steps
Ethyl 2-(2-t-pentyloxycarbonylamino-1,3-thiazol-4-yl)-acetate (0.3 g.) and selenium dioxide (0.11 g.) were treated according to a similar manner to that of Preparation 6-4) to give brown oil of ethyl 2-(2-t-pentyloxycarbonylamino-1,3-thiazol-4-yl)glyoxylate (0.22 g.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04431643 |
| Source dataset | uspto-grants-1984_02 |
| ORD ID | ord-2fceab964178486aa94ec3f4defe3296 |
| Source note | uspto-grants-1984_02 |